1,6,7,12-四氯-3,4,9,10-苝四甲酸二酐合成路线 （共 4 条）
反应条件
sulfuric acid; chlorine T=120°C;
参考文献
Journal of the American Chemical Society, , vol. 130, # 26 p. 8271 - 8279
反应条件
chlorosulfonic acid; iodine T=70°C; 5 h;
参考文献
Tetrahedron, , vol. 68, # 2 p. 722 - 729
反应条件
chlorosulfonic acid; iodine T=70°C; 20 h;
参考文献
Tetrahedron, , vol. 68, # 2 p. 722 - 729
反应条件
1.1: propionic acid / Reflux 2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 14 h / 130 °C / Inert atmosphere 3.1: potassium hydroxide / tert-butyl alcohol / Heating 3.2: Acidic aq. solution View Scheme
参考文献
Perrin, Lara; Hudhomme, Pietrick
European Journal of Organic Chemistry, 2011 , # 28 p. 5427 - 5440
