1,6,7,12-四叔丁基苯氧基苝-3,4,9,10-四甲酸二酐合成路线 （共 9 条）
反应条件
potassium hydroxide in tert-butyl alcohol T=80°C; 10 h;
参考文献
Wuerthner, Frank; Thalacker, Christoph; Sautter, Armin; Schaertl, Wolfgang; Ibach, Wolfram; Hollricher, Olaf
Chemistry - A European Journal, 2000 , vol. 6, # 21 p. 3871 - 3886
反应条件
lithium hydroxide in tert-butyl alcohol Reflux;
参考文献
Baffreau, Jerome; Leroy-Lhez, Stephanie; Anh, Nguyen Van; Williams, Rene M.; Hudhomme, Pietrick
Chemistry - A European Journal, 2008 , vol. 14, # 16 p. 4974 - 4992
反应条件
potassium hydroxide in water; isopropyl alcohol 24 h; Inert atmosphereReflux;
参考文献
Kim, Ki-Soo; Jeong, Seonju; Kim, Cham; Kim, Hoyoung; Yang, Yu Suk; Kim, Jae Hong; Kwon, Younghwan; Tai, Weon-Pil; Han, Yoon Soo
Molecular Crystals and Liquid Crystals, 2010 , vol. 532, p. 29 - 38
反应条件
1.1: propan-1-ol; water / 12 h / 65 °C / Inert atmosphere 2.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 14 h / 80 °C / Inert atmosphere 2.2: 6 h / Inert atmosphere 3.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 160 °C / Inert atmosphere 4.1: potassium hydroxide / water; isopropyl alcohol / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Molecular Crystals and Liquid Crystals, , vol. 532, p. 29 - 38
反应条件
potassium hydroxide; water in isopropyl alcohol 13 h; Reflux;
参考文献
Organic and Biomolecular Chemistry, , vol. 6, # 7 p. 1268 - 1277
反应条件
1.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 14 h / 130 °C / Inert atmosphere 2.1: potassium hydroxide / tert-butyl alcohol / Heating 2.2: Acidic aq. solution View Scheme
参考文献
European Journal of Organic Chemistry, , # 28 p. 5427 - 5440
反应条件
1.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 8 h / 80 - 85 °C 2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 14 h / 130 °C / Inert atmosphere 3.1: potassium hydroxide / tert-butyl alcohol / Heating 3.2: Acidic aq. solution View Scheme
参考文献
European Journal of Organic Chemistry, , # 28 p. 5427 - 5440
反应条件
1.1: propionic acid / Reflux 2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 14 h / 130 °C / Inert atmosphere 3.1: potassium hydroxide / tert-butyl alcohol / Heating 3.2: Acidic aq. solution View Scheme
参考文献
European Journal of Organic Chemistry, , # 28 p. 5427 - 5440
反应条件
1.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 14 h / 80 °C / Inert atmosphere 1.2: 6 h / Inert atmosphere 2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 160 °C / Inert atmosphere 3.1: potassium hydroxide / water; isopropyl alcohol / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Molecular Crystals and Liquid Crystals, , vol. 532, p. 29 - 38
