1,1,1,9-四氯壬烷合成路线 （共 16 条）
反应条件
2,2'-azo-bisisobutyronitrile T=90°C; P=88260.9 Torr;
参考文献
Joyce; Hanford; Harmon
Journal of the American Chemical Society, 1948 , vol. 70, p. 2531
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2440800 , 1942 ;
反应条件
T=95°C; P=73550.8 Torr;
参考文献
Kharasch; Jensen; Urry
Journal of the American Chemical Society, 1947 , vol. 69, p. 1104
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2396261 ;
反应条件
dicyclohexyl peroxydicarbonate
参考文献
Chukovskaya,E.Ts. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1965 , p. 445 - 449
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1965 , # 3 p. 461 - 465
反应条件
hexacarbonyl chromium T=120°C; relative rate of telomerization initiated by Cr(CO)6 and further initiator; partial chain-transfer constants; Product distribution;
参考文献
Grigor'ev, N. A.; Tumanskaya, A. L.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 187 - 190
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 199 - 202
反应条件
1: 91 percent / 93percent H2SO4 2: 96 percent / aq. NaOH / 7 h / Heating View Scheme
参考文献
Saotome,K. et al.
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, p. 480 - 484
反应条件
1: 91 percent / 93percent H2SO4 2: 96 percent / aq. NaOH / 7 h / Heating 3: 94 percent / H2SO4 View Scheme
参考文献
Zakharkin, L. I.; Zhigareva, G. G.; Podvisotskaya, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2574 - 2575
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2809 - 2810
反应条件
1: 91 percent / 93percent H2SO4 2: 96 percent / aq. NaOH / 7 h / Heating 3: 93 percent / H2SO4 / Heating View Scheme
参考文献
Zakharkin, L. I.; Zhigareva, G. G.; Podvisotskaya, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2574 - 2575
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2809 - 2810
反应条件
1: HNO3, NO2 2: Na / methanol / (electrolysis) 3: dimethylformamide 4: H2SO4, Ac2O / H2O / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 39, p. 480 - 484
反应条件
1: HNO3, NO2 2: aq. NaOH / Heating 3: Na / methanol / (electrolysis) View Scheme
参考文献
Saotome,K. et al.
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, p. 480 - 484
反应条件
1: HNO3, NO2 2: aq. NaOH / Heating 3: Na / methanol / (electrolysis) 4: KMnO4 / acetone; H2O / 70 °C View Scheme
参考文献
Saotome,K. et al.
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, p. 480 - 484
