1,1,1,9-四氯壬烷合成路线 （共 16 条）
反应条件
1: HNO3, NO2 2: Na / methanol / (electrolysis) 3: dimethylformamide 4: H2, NH3 / Raney-Ni / methanol View Scheme
参考文献
Saotome,K. et al.
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, p. 480 - 484
反应条件
1: antimony (V)-chloride 2: aqueous 2-methoxy-ethanol / 120 °C 3: lithium alanate; diethyl ether 4: aqueous H2SO4 View Scheme
参考文献
Nesmejanow et al.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2418,2422;engl.Ausg.S.2481,2484
反应条件
ammonia; hydrogen; palladium on barium sulfate in methanol; acetic acid
参考文献
Freidlina,R.Kh.; Kost,T.A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1960 , p. 1291 - 1293
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , # 8 p. 1387 - 1390
反应条件
1: 91 percent / 93percent H2SO4
2: 96 percent / aq. NaOH / 7 h / Heating
3: 93 percent / H2SO4 / Heating
4: 71 percent / pyridinium chlorochromate / CH2Cl2
View Scheme
参考文献
Zakharkin, L. I.; Zhigareva, G. G.; Podvisotskaya, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2574 - 2575
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2809 - 2810
参考文献
Zakharkin, L. I.; Zhigareva, G. G.; Podvisotskaya, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2574 - 2575
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2809 - 2810
反应条件
1: HNO3, NO2
2: Na / methanol / (electrolysis)
View Scheme
参考文献
Saotome,K. et al.
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, p. 480 - 484
