反应条件
1,3-bis-(diphenylphosphino)propane in benzene stirring (30 min, N2-atmosphere); pptn. on pentane addn., filtration, washing (pentane), drying (vac., room temp.), dissoln. in DMF (85°C), filtration, cooling, Et2O addn., crystn. (ice bath);
参考文献
Komoroski, Richard A.; Magistro, Angelo J.; Nicholas, Paul P.
Inorganic Chemistry, 1986 , vol. 25, p. 3917 - 3925