(5Z)-5-(3-溴亚丙基)-5,11-二氢-10H-二苯并[a,d]环庚烯-10-醇合成路线 （共 5 条）
反应条件
sodium tetrahydroborate in methanol 1 h; Ambient temperature;
参考文献
Jean-Claude; Just
Synthetic Communications, 1994 , vol. 24, # 11 p. 1565 - 1573
反应条件
1: 1.) BuLi / 1.) THF, hexane, from -80 deg C to RT, 2.) THF, hexane, RT, 4 h 2: 100 percent / 0.1N HCl / methanol / 6 h 3: 67 percent / CBr4, PPh3 / CH2Cl2 / 2 h / 0 °C 4: 100 percent / NaBH4 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Jean-Claude; Just
Synthetic Communications, 1994 , vol. 24, # 11 p. 1565 - 1573
反应条件
1: 67 percent / CBr4, PPh3 / CH2Cl2 / 2 h / 0 °C 2: 100 percent / NaBH4 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Jean-Claude; Just
Synthetic Communications, 1994 , vol. 24, # 11 p. 1565 - 1573
反应条件
1: 48percent HBr / acetic acid / Heating 2: 100 percent / NaBH4 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 24, # 11 p. 1565 - 1573
反应条件
1: 100 percent / 0.1N HCl / methanol / 6 h 2: 67 percent / CBr4, PPh3 / CH2Cl2 / 2 h / 0 °C 3: 100 percent / NaBH4 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Jean-Claude; Just
Synthetic Communications, 1994 , vol. 24, # 11 p. 1565 - 1573
