S-(-)-2-甲基-1-丁醇合成路线 （共 117 条）
反应条件
1: With oxygen; ozone in methanol T=-78°C; 0.166667 h; 2: With sodium tetrahydroborate in methanol T=-78 - 20°C; 4.5 h;
参考文献
Tetrahedron, , vol. 69, # 36 p. 7785 - 7809
反应条件
1: With oxygen; ozone in methanol T=-78°C; 0.166667 h; 2: With sodium tetrahydroborate in methanol T=-78 - 20°C; 3.5 h;
参考文献
Tetrahedron, , vol. 69, # 36 p. 7785 - 7809
反应条件
methanol; lithium aluminium tetrahydride in tetrahydrofuran 4 h; Heating;
参考文献
Bestmann, Hans Juergen; Frighetto, Rosa T. S.; Frighetto, Nelson; Vostrowsky, Otto
Liebigs Annalen der Chemie, 1988 , p. 877 - 880
反应条件
ethanol; nickel T=145 - 150°C; P=73550.8 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1964
Journal of the American Chemical Society, , vol. 67, p. 1352
反应条件
1: With hydrogen; N-heterocyclic carbene complex in dichloromethane T=25°C; P=15201 Torr; 4 h; 2: With lithium aluminium tetrahydride Further stages. Title compound not separated from byproducts.;
参考文献
Chemistry - A European Journal, , vol. 13, # 25 p. 7162 - 7170
反应条件
1: With hydrogen; N-heterocyclic carbene complex in dichloromethane T=25°C; P=15201 Torr; 4 h; 2: With lithium aluminium tetrahydride Further stages. Title compound not separated from byproducts.;
参考文献
Chemistry - A European Journal, , vol. 13, # 25 p. 7162 - 7170
反应条件
hydrogen; N-heterocyclic carbene complex in dichloromethane T=25°C; P=15201 Torr; 4 h; Title compound not separated from byproducts.;
参考文献
Chemistry - A European Journal, , vol. 13, # 25 p. 7162 - 7170
反应条件
1: With (R,R,R,R)-(-)-trans,trans-2,3,10,11-tetrakis(hydroxydiphe.. T=20°C; inclusion complexation; resolution of racemate; 24 h; 2: T=180°C; decomposition of complex; P=30 Torr;
参考文献
Tanaka, Koichi; Honke, Shinji; Urbanczyk-Lipkowska, Zofia; Toda, Fumio
European Journal of Organic Chemistry, 2000 , # 18 p. 3171 - 3176
反应条件
pyridinium p-toluenesulfonate in ethanol 12 h; Ambient temperature;
参考文献
Mori, Kenji; Wu, Jiang
Liebigs Annalen der Chemie, 1991 , # 3 p. 213 - 217
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Ambient temperature;
参考文献
Gaucher, Anne; Ollivier, Jean; Marguerite, Jacqueline; Paugam, Renee; Salauen, Jacques
Canadian Journal of Chemistry, 1994 , vol. 72, # 5 p. 1312 - 1327
