S-(-)-2-甲基-1-丁醇合成路线 （共 117 条）
反应条件
active pentyl butyrate;
参考文献
Walden
Zeitschrift fuer Physikalische Chemie, Stoechiometrie und Verwandtschaftslehre, 1896 , vol. 20, p. 573
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1898 , vol. 30, p. 774
Chem. Zentralbl., 1899 , vol. 70, # I p. 327
反应条件
am Rueckflusskuehler; active pentyl butyrate;
参考文献
Minguin
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 947
反应条件
pyridine T=4°C; 12 h;
参考文献
Mori, Kenji
Tetrahedron, 2009 , vol. 65, # 19 p. 3900 - 3909
反应条件
1: PCC, Al / CHCl3 / 2 h / Ambient temperature 2: 76 percent / aq. NaOH / dimethylformamide / 2 h / -10 - 5 °C 3: 45 percent / aq, NaOH, NaN3 / 1,2-dimethoxy-ethane / 24 h / Ambient temperature 4: 1.) H2, 2.) aq. NaOH / 1.) Pd-C / 1.) ethyl acetate, MeOH, 18 h, 2.) 0 deg C, 90 min View Scheme
参考文献
Lloyd-Williams, Paul; Monerris, Patricia; Gonzalez, Isabel; Jou, Gemma; Giralt, Ernest
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 14 p. 1969 - 1974
反应条件
1: pyridine 2: NaN3 / dimethylformamide 3: LiAlH4 / diethyl ether View Scheme
参考文献
Anteunis, M. J. O.; Callens, R.; Witte, M. De; Reyniers, M. F.; Spiessens, L.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 7 p. 545 - 554
反应条件
hydrogen iodide dextrorotatory form of 1-iodo-2-methylbutane;
参考文献
Just
Justus Liebigs Annalen der Chemie, 1883 , vol. 220, p. 150
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Le Bel
Bulletin de la Societe Chimique de France, 1876 , vol. <2>25, p. 545
Bulletin de la Societe Chimique de France, 1874 , vol. <2>21, p. 542
Full Text Show Details
Klages; Sautter
Chemische Berichte, 1904 , vol. 37, p. 654
反应条件
carbon tetrabromide; triphenylphosphine in benzene 3 h; Heating;
参考文献
Anteunis, M. J. O.; Callens, R.; Witte, M. De; Reyniers, M. F.; Spiessens, L.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 7 p. 545 - 554
参考文献
Nozakura,S. et al.
Bulletin of the Chemical Society of Japan, 1961 , vol. 34, p. 1673 - 1678
反应条件
1: pyridine 2: dimethylformamide 3: 40 percent aq. KOH View Scheme
参考文献
Black,D.K.; Landor,S.R.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 288 - 290
反应条件
(i) PBr3, (ii) Mg, (iii) /BRN= 1900390/; Multistep reaction;
参考文献
Potapov,V.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1972 , vol. 8, p. 953 - 957
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, p. 948 - 953
