5-((2S,3S)-3-((R)-1-(叔丁基二甲基甲硅烷基氧基)乙基)-4-氧代氮杂啶-2-基)-2,2,5-三甲基-1,3-二噁烷-4,6-二酮合成路线 （共 6 条）
反应条件
triethylamine in ethyl acetate T=65°C; 4 h;
参考文献
Choi, Woo-Baeg; Churchill, Hywyn R. O.; Lynch, Joseph E.; Thompson, Andrew S.; Humphrey, Guy R.; Volante; Reider, Paul J.; Shinkai, Ichiro
Tetrahedron Letters, 1994 , vol. 35, # 15 p. 2275 - 2278
反应条件
triethylamine in ethyl acetate T=70°C; 5 h;
参考文献
Laurent, Mathieu; Ceresiat, Marcel; Marchand-Brynaert, Jacqueline
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 3194 - 3197
反应条件
1: 95 percent / imidazole / dimethylformamide / 48 h / 20 °C 2: 0.024 g / Et3N / ethyl acetate / 5 h / 70 °C View Scheme
参考文献
Laurent, Mathieu; Ceresiat, Marcel; Marchand-Brynaert, Jacqueline
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 3194 - 3197
反应条件
1: 95 percent / imidazole / dimethylformamide / 48 h / 20 °C 2: 0.024 g / Et3N / ethyl acetate / 5 h / 70 °C View Scheme
参考文献
Laurent, Mathieu; Ceresiat, Marcel; Marchand-Brynaert, Jacqueline
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 3194 - 3197
反应条件
1: 95 percent / NaI, Et3N / dimethylformamide / 3 h / 60 °C 2: 1.) CH3O(1-) View Scheme
参考文献
Choi, Woo-Baeg; Churchill, Hywyn R. O.; Lynch, Joseph E.; Thompson, Andrew S.; Humphrey, Guy R.; Volante; Reider, Paul J.; Shinkai, Ichiro
Tetrahedron Letters, 1994 , vol. 35, # 15 p. 2275 - 2278
反应条件
triethylamine; sodium iodide in N,N-dimethyl-formamide T=60°C; 3 h;
参考文献
Choi, Woo-Baeg; Churchill, Hywyn R. O.; Lynch, Joseph E.; Thompson, Andrew S.; Humphrey, Guy R.; Volante; Reider, Paul J.; Shinkai, Ichiro
Tetrahedron Letters, 1994 , vol. 35, # 15 p. 2275 - 2278
