1: With sec.-butyllithium in tetrahydrofuran; hexane T=-78°C; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane 3: With hydrogenchloride in tetrahydrofuran; hexane 0.166667 h;
参考文献
Mewshaw, Richard E.; Edsall Jr., Richard J.; Yang, Cuijian; Manas, Eric S.; Xu, Zhang B.; Henderson, Ruth A.; Keith Jr., James C.; Harris, Heather A.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 12 p. 3953 - 3979
1: 2-methoxy-6-bromo-naphthalene With magnesium in tetrahydrofuran 1 h; 2: boron triethoxide in tetrahydrofuran T=-78°C; 10 h; 3: With hydrogenchloride in tetrahydrofuran; water
参考文献
GYEONGSANG NATIONAL UNIVERSITY INDUSTRIAL AND ACADEMIC COLLABORATION FOUNDATION
Patent: WO2008/120839 A1, 2008 ;
Location in patent: Page/Page column 47-48 ;
potassium phosphate; SK-CC02-A in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; 19 h;
参考文献
Gogsig, Thomas M.; Sobjerg, Lina S.; Lindhardt, Anders T.; Jensen, Kim L.; Skrydstrup, Troels
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3404 - 3410
