5-(乙酰氨基)-5-脱氧-3-S-苯基-3-硫代-D-赤式-alpha-L-葡糖-2-吡喃壬酮糖酸甲酯2,4,7,8,9-五乙酸酯合成路线 （共 2 条）
反应条件
Multi-step reaction with 4 steps 1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 6 h / 0 °C2: 57 percent / CH2Cl2 / 168 h / 20 °C3: HgBr2, Hg(CN)2 / 1,2-dichloro-ethane; H2O / 3.5 h / Heating4: pyridine, DMAP / 1 h / 20 °C
参考文献
Ercegovic, Teddy; Magnusson, Goeran Journal of the Chemical Society, Chemical Communications, 1994 , # 7 p. 831 - 832
反应条件
Multi-step reaction with 2 steps 1: HgBr2, Hg(CN)2 / 1,2-dichloro-ethane; H2O / 3.5 h / Heating2: pyridine, DMAP / 1 h / 20 °C
参考文献
Ercegovic, Teddy; Magnusson, Goeran Journal of the Chemical Society, Chemical Communications, 1994 , # 7 p. 831 - 832
