反应条件
1.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0.08 h / 20 °C 1.2: 20 °C 2.1: sodium t-butanolate / tetrahydrofuran / 0.42 h / 0 - 5 °C 2.2: 20 °C 3.1: trimethyl-tin hydroxide / 1,2-dichloro-ethane / 0.5 h / 130 °C / |Inert atmosphere; |Microwave irradiation View Scheme
参考文献
Liedtke, Andy J.; Marnett, Lawrence J.; Kim, Kwangho; Stec, Donald F.; Sulikowski, Gary A.
Tetrahedron, 2012 , vol. 68, # 48 p. 10049 - 10058,10
Title/Abstract Full Text Show Details
Liedtke, Andy J.; Kim, Kwangho; Stec, Donald F.; Sulikowski, Gary A.; Marnett, Lawrence J.
Tetrahedron, 2012 , vol. 68, # 48 p. 10049 - 10058