3-(2-噻吩基)丙烯酸合成路线 （共 20 条）
反应条件
[bmim]PF6; triethylamine; bis-triphenylphosphine-palladium(II) chloride in water T=100°C; P=15001.2 Torr; 20 h;
参考文献
Zhao, Xiaodan; Alper, Howard; Yu, Zhengkun
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3988 - 3990
反应条件
triethylamine; di-(3-methylphenyl)phosphinopolystyrene palladium catalyst in acetonitrile T=80°C; Heck cross-coupling reaction; 20 h;
参考文献
Schweizer, Stephane; Becht, Jean-Michel; Le Drian, Claude
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1150 - 1158
反应条件
ammonium acetate 0.05 h; Irradiation;
参考文献
Sampath Kumar; Subbareddy; Anjaneyulu; Yadav
Synthetic Communications, 1998 , vol. 28, # 20 p. 3811 - 3815
反应条件
potassium hydroxide; PS-PEG-NH-C(O)C6H4PPh2-PdCl(η3-C3H5) T=50°C; Heck reaction;
参考文献
Uozumi, Yasuhiro; Kimura, Tsutomu
Synlett, 2002 , # 12 p. 2045 - 2048
反应条件
zinc dibromide in tetrahydrofuran 32 h; Ambient temperature;
参考文献
Bellassoued, Moncef; Lensen, Nathalie; Bakasse, Mina; Mouelhi, Sinda
Journal of Organic Chemistry, 1998 , vol. 63, # 24 p. 8785 - 8789
反应条件
palladium dichloride in water Heck reaction; 0.00555556 h; microwave irradiation;
参考文献
Zhu, Min; Song, Yunlong; Cao, Yan
Synthesis, 2007 , # 6 p. 853 - 856
反应条件
FeCl3·6H2O; water in nitromethane T=110°C; 0.75 h; Sealed tube; Overall yield = 87 percent; Overall yield = 114 mg;
参考文献
Organic Letters, , vol. 15, # 17 p. 4564 - 4567
反应条件
ammonium acetate in ethanol Rodionov reaction; 12 h; Heating;
参考文献
Russian Journal of General Chemistry, , vol. 75, # 7 p. 1113 - 1124
反应条件
potassium hydroxide 4 h; Heating;
参考文献
Paizs, Csaba; Katona, Adrian; Retey, Janos
Chemistry - A European Journal, 2006 , vol. 12, # 10 p. 2739 - 2744
反应条件
1: water / 2 h / 75 °C 2: FeCl3·6H2O; water / nitromethane / 0.75 h / 110 °C / |Sealed tube View Scheme
参考文献
Organic Letters, , vol. 15, # 17 p. 4564 - 4567
