反应条件
in further solvent(s)
inert atmosphere; heating Os-complex with excess PMe3 (in p-xylene, closed vessel, 130°C, 6 h); solvent removal (vac.), sublimation off of mononuclear complexes (20-90°C, 9.8E-3 Torr) and/or chromy. (SiO2, hexane/CH2Cl2), recrystn. (hexane/CH2Cl2); elem. anal.;
参考文献
Male, Jonathan L.; Einstein, Frederick W. B.; Leong, Weng K.; Pomeroy, Roland K.; Tyler, David R.
Journal of Organometallic Chemistry, 1997 , vol. 549, # 1-2 p. 105 - 115