反应条件
hydrogen in octane
Os3(CO)12 refluxed in octane with (CpNi(CO))2 for 30 min under H2 flow,cooled; filtered, evapd. in vac., purified by TLC (Kiselgel PF Merck, light petroleum-Et2O), crystd. from CHCl3/heptane at -10°C; elem. anal.;
参考文献
Castiglioni, Mario; Sappa, Enrico; Valle, Mario; Lanfranchi, Maurizio; Tiripicchio, Antonio
Journal of Organometallic Chemistry, 1983 , vol. 241, # 1 p. 99 - 112
