反应条件
in neat (no solvent) heating in a sealed Carius tube in vacuo to 205°C for 20 min; cooling to room temp., opening, addn. of CH2Cl2, Os3(CO)12 is filtered off, evapn., drying on Florisil, chromy. (Florisil, heptane), concg., addn. of seed crystal, crystn. at -10°C; elem. anal.;
参考文献
Organometallics, , vol. 7, p. 969 - 977
