反应条件
in dichloromethane under N2, Me3NO in CH2Cl2 was added dropwise to CH2Cl2 soln. of Os-complex (molar ratio was 2:1), stirring at room temp. for 20 h; solvent was removed in vac., chromy. on silica, elution with hexane/CH2Cl2 (7:3, v/v), recrystd. from hexane/CH2Cl2 at -20 °C;
参考文献
Polyhedron, , vol. 19, # 9 p. 1081 - 1084
