3,4-二(苄氧基)苯甲酸合成路线 (共 25 条)
反应条件
potassium hydroxide in ethanol; water 1 h; Heating;
参考文献
Tranchimand, Sylvain; Tron, Thierry; Gaudin, Christian; Iacazio, Gilles
Synthetic Communications, 2006 , vol. 36, # 5 p. 587 - 597
反应条件
potassium hydroxide in tetrahydrofuran; water 48 h;
参考文献
Schmidt, Rolf; Carrigan, Joseph G.; DeWolf, Christine E.
Canadian Journal of Chemistry, 2006 , vol. 84, # 10 p. 1411 - 1415
反应条件
1: With potassium carbonate in acetone Reflux; 2: With sodium hydroxide in methanol; water 2 h; Reflux;
参考文献
Wang, Wen-Long; Chai, Sergio C.; Ye, Qi-Zhuang
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 4 p. 1080 - 1083
反应条件
potassium permanganate in water; acetone 6.5 h; Heating;
参考文献
Hu, Hong; Mendoza, Jose S.; Lowden, Christopher T.; Ballas, Lawrence M.; Janzen, William P.
Bioorganic and Medicinal Chemistry, 1997 , vol. 5, # 9 p. 1873 - 1882
参考文献
WAKO PURE CHEMICAL INDUSTRIES LTD; MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD.
Patent: EP636941 A1, 1995 ;
反应条件
potassium hydroxide in methanol; water; butanone
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4798892 A1, 1989 ;
反应条件
potassium hydroxide in pyridine; diethylene glycol T=120°C; Ring cleavage; 6 h;
参考文献
Caldwell, Stuart T.; Crozier, Alan; Hartley, Richard C.
Tetrahedron, 2000 , vol. 56, # 24 p. 4101 - 4106
反应条件
1: 73 percent / H2SO4 / 168 h / Heating 2: 77 percent / K2CO3 / CH2Cl2; methanol / 6 h 3: 95 percent / KOH / tetrahydrofuran; H2O / 48 h View Scheme
参考文献
Bugdahn, Nikolas; Peuckert, Florian; Albrecht, Alexander G.; Miethke, Marcus; Marahiel, Mohamed A.; Oberthuer, Markus
Angewandte Chemie - International Edition, 2010 , vol. 49, # 52 p. 10210 - 10213
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; Oxidation;
参考文献
Iakovidis, Dimitri; Louis, Simon N. S.; Rezmann, Linda A.; Colagrande, Felicia; Nero, Tracy L.; Jackman, Graham P.; Louis, William J.
European Journal of Medicinal Chemistry, 1999 , vol. 34, # 6 p. 539 - 548
反应条件
1: 77 percent / K2CO3 / CH2Cl2; methanol / 6 h 2: 95 percent / KOH / tetrahydrofuran; H2O / 48 h View Scheme
参考文献
Astles; Brown; Handscombe; Harper; Harris; Lewis; Lockey; McCarthy; McLay; Porter; Roach; Smith; Walsh
European Journal of Medicinal Chemistry, 1997 , vol. 32, # 5 p. 409 - 423