3,4-二(苄氧基)苯甲酸合成路线 （共 25 条）
反应条件
sodium hydroxide in methanol; water 3 h; Heating;
参考文献
Gardner, Richard Andrew; Kinkade, Rebecca; Wang, Chaojie; Phanstiel IV, Otto
Journal of Organic Chemistry, 2004 , vol. 69, # 10 p. 3530 - 3537
反应条件
1: K2CO3*1.5H2O / acetone / 24 h / Heating 2: 1.93 g / NaOH / H2O; methanol / 3 h / Heating View Scheme
参考文献
Gardner, Richard Andrew; Kinkade, Rebecca; Wang, Chaojie; Phanstiel IV, Otto
Journal of Organic Chemistry, 2004 , vol. 69, # 10 p. 3530 - 3537
反应条件
1: K2CO3*1.5H2O / acetone / 24 h / Heating 2: 1.93 g / NaOH / H2O; methanol / 3 h / Heating View Scheme
参考文献
Lee, Seokwoo; Hwang, Soonho; Yu, Shuai; Jang, Wonyoung; Lee, Yun Mi; Kim, Sanghee
Archives of Pharmacal Research, 2011 , vol. 34, # 7 p. 1065 - 1070
反应条件
1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / Inert atmosphere 2: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; acetonitrile; tert-butyl alcohol / 0.17 h / 20 °C / Inert atmosphere View Scheme
参考文献
Lee, Seokwoo; Hwang, Soonho; Yu, Shuai; Jang, Wonyoung; Lee, Yun Mi; Kim, Sanghee
Archives of Pharmacal Research, 2011 , vol. 34, # 7 p. 1065 - 1070
参考文献
Shimizu; Ohta
Yakugaku Zasshi, 1951 , vol. 71, p. 1485,1487
Chem.Abstr., 1952 , p. 7099
参考文献
Priestley; Moness
Journal of Organic Chemistry, 1940 , vol. 5, p. 355,358
参考文献
Priestley; Moness
Journal of Organic Chemistry, 1940 , vol. 5, p. 355,358
反应条件
1: (i) SOCl2, benzene, (ii) aq. NH3 2: H2 / Pd-C / acetic acid View Scheme
参考文献
Carlsson,A. et al.
Helvetica Chimica Acta, 1962 , vol. 45, p. 270 - 276
反应条件
thionyl chloride; N,N-dimethyl-formamide 6 h; Heating;
参考文献
Boers, Frank; Deng, Bo-Liang; Lemiere, Guy; Lepoivre, Jozef; De Groot, Alex; Dommisse, Roger; Vlietinck, Arnold J.
Archiv der Pharmazie, 1997 , vol. 330, # 9-10 p. 313 - 316
反应条件
1.1: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere 1.2: 2 h / Reflux; Inert atmosphere 2.1: potassium hydroxide / ethanol / 18 h / Reflux; Inert atmosphere View Scheme
参考文献
Lee, Seokwoo; Hwang, Soonho; Yu, Shuai; Jang, Wonyoung; Lee, Yun Mi; Kim, Sanghee
Archives of Pharmacal Research, 2011 , vol. 34, # 7 p. 1065 - 1070
