2-苯基-1,3-丙二醇合成路线 （共 45 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Hylands, Kevin A.; Moodie, Roy B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 10 p. 2073 - 2078
反应条件
lithium aluminium tetrahydride
参考文献
Virtanen, Terttu; Nikander, Hannu
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 2 p. 113 - 116
反应条件
1,3-disubstituted tetraalkyldistannoxane (X = Y = Cl) in methanol; chloroform 48 h; Ambient temperature; Yield given;
参考文献
Tetrahedron, , vol. 49, # 15 p. 3065 - 3074
反应条件
water in methanol T=20°C; Irradiation; Quantum yield;
参考文献
Kostikov, Alexey P.; Popik, Vladimir V.
Organic Letters, 2008 , vol. 10, # 22 p. 5277 - 5280
反应条件
T=150°C; P=257428 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 3121
反应条件
aluminium trichloride
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 991,993; engl. Ausg. S. 965
反应条件
acetate buffer pH 5 in water T=30°C; 168 h; Gluconobacter roseus IAM 1841;
参考文献
Ohta, Hiromichi; Tetsukawa, Hatsuki; Noto, Naoko
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2400 - 2404
反应条件
1: in tetrahydrofuran 2: With (NH4)2CO3 in tetrahydrofuran 38 - 72 h; Molecular sieve;
参考文献
Mortko, Henry; He, Weixuan; Andersen, Marc W.; Dotse, Anthony K.; Li, Jie
Patent: US2006/241298 A1, 2006 ;
Location in patent: Page/Page column 8 ;
反应条件
1: in tetrahydrofuran T=20°C; 1 h; 2: With ammonia in tetrahydrofuran T=-48°C; 3 h;
参考文献
Thompson, Charles D.; Gulden, Pamela H.; Macdonald, Timothy L.
Chemical Research in Toxicology, 1997 , vol. 10, # 4 p. 457 - 462
反应条件
1: 1.) sodium hydride / 1.) DMSO, RT, 5 h, 2.) RT, overnight 2: tetrahydrofuran / 2 h / Ambient temperature 3: ammonia / toluene / 0.5 h / 0 °C 4: 96 percent / trichloromethylsilane, sodium iodide / acetonitrile / 24 h / Ambient temperature View Scheme
参考文献
Choi; Kucharczyk; Sofia
Tetrahedron, 1986 , vol. 42, # 23 p. 6399 - 6404
