2-(3,5-二氟苯基)乙酰氯合成路线 (共 5 条)
反应条件
oxalyl dichloride in dichloromethane; N,N-dimethyl-formamide T=20°C; Chlorination; 1 h;
参考文献
Tetrahedron, , vol. 55, # 19 p. 6001 - 6018
反应条件
in dichloromethane; N,N-dimethyl-formamide
参考文献
US6506782 B1, ;
US6509331 B1, ;
反应条件
AlCl3, aluminium chloride
参考文献
DAINIPPON INK AND CHEMICALS, INC.
Patent: EP1191008 A1, 2002 ;
Location in patent: Page 68 ;
反应条件
sodium hydroxide in water T=0 - 20°C; Schotten-Baumann Reaction;
参考文献
EP951466 B1, ;
Page/Page column 64 ;
反应条件
in sodium hydroxide; ethyl acetate
参考文献
US6486350 B1, ;
US 6486350 B1