ALPHA-D-赤式戊呋喃糖-2-酮 1,3,5-三苯甲酸酯合成路线 （共 11 条）
反应条件
titanium tetrachloride 1.) ether, -78 deg.C; 2.) ether, 4 h, -30 - -40 deg.C; Multistep reaction;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
Title compound not separated from byproducts;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
4-(N,N-dimethlyamino)pyridine; titanium tetrachloride; triethylamine Yield given. Multistep reaction;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine Yield given. Multistep reaction;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
1: 1.) CeCl3, 2.) DMAP, Et3N 2: bis(trimethylsilyl)acetamide, SnCl4 / acetonitrile / 3 h / Heating 3: NH3/MeOH View Scheme
参考文献
Wolfe; Harry-O'kuru
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7611 - 7614
反应条件
4-(N,N-dimethlyamino)pyridine; titanium tetrachloride; triethylamine Yield given. Multistep reaction;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine Yield given. Multistep reaction;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
1: 1.) CeCl3, 2.) DMAP, Et3N 2: 47 percent / bis(trimethylsilyl)acetamide, TMSOTf / acetonitrile / Heating 3: NH3/MeOH View Scheme
参考文献
Wolfe; Harry-O'kuru
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7611 - 7614
反应条件
titanium tetrachloride 1.) ether, -78 deg.C; 2.) ether, 4 h, -30 - -40 deg.C; Multistep reaction;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
Title compound not separated from byproducts;
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
