1: toluene / 15.5 h / Heating 2: NaBH4 / tetrahydrofuran; methanol / 20 h / 20 °C View Scheme
参考文献
Ashton, Peter R.; Glink, Peter T.; Stoddart, J. Fraser; Tasker, Peter A.; White, Andrew J. P.; Williams, David J.
Chemistry--A European Journal, 1996 , vol. 2, # 6 p. 729 - 736
1: With toluene-4-sulfonic acid in toluene 1 h; Dean-Stark conditions; 2: With bis(2-methoxyethoxy)aluminum hydride in toluene T=22°C; 3: With water; Sodium potassium tartrate in toluene 1 h;
1: With dicarbonyl(pentamethylcyclopentadienyl)(4-methoxyphenyl)iron in dichloromethane 4 h; Inert atmosphereIrradiationSchlenk technique; 2: With sodium hydroxide in methanol; water Schlenk techniqueInert atmosphere;
