反应条件
1-propanol in methanol; benzene
byproducts: H2O; di-n-butyltin oxide refluxed with PrOH for 4 h; azeotrope (C6H6/H2O/PrOH) removed; mixt. cooled to room temp.; soln. of MePO(OH)2 in molar ratio1:2 in benzene and MeOH slowly added; stirred at room temp. for 18 h; filtered off; solvent removed (vac.); elem. anal.;
参考文献
Ribot, Francois; Sanchez, Clement; Biesemans, Monique; Mercier, Frederic A. G.; Martins, Jose C.; Gielen, Marcel; Willem, Rudolph
Organometallics, 2001 , vol. 20, # 12 p. 2593 - 2603
