2',3',5-三-O-乙酰基-8-溴鸟苷合成路线 （共 6 条）
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin in acetonitrile T=25°C; 4 h;
参考文献
Rayala, Ramanjaneyulu; Wnuk, Stanislaw F.
Tetrahedron Letters, 2012 , vol. 53, # 26 p. 3333 - 3336
反应条件
in pyridine 1 h; Ambient temperature;
参考文献
Schulz, Bernd S.; Pfleiderer, Wolfgang
Helvetica Chimica Acta, 1987 , vol. 70, p. 210 - 218
反应条件
2-(N,N-dimethylamino)-pyridine; acetic anhydride; triethylamine in acetonitrile
参考文献
US2013/52710 A1, ;
Page/Page column ;
反应条件
bromination reagent Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 26, # 44 p. 5421 - 5424
反应条件
methanol; water; triethylamine T=71°C; Microwave irradiation;
参考文献
Meier, Lidiane; Monteiro, Gustavo C.; Baldissera, Rodrigo A.M.; Sa, Marcus Mandolesi
Journal of the Brazilian Chemical Society, 2010 , vol. 21, # 5 p. 859 - 866
反应条件
1: 93 percent / H3PO4 / 1 h / 100 °C
2: K2CO3 / dimethylformamide / 24 h / Ambient temperature
3: 76 percent / CH3NH2, H2O / 3 h / Ambient temperature
View Scheme
参考文献
Madre, Marina; Panchenko, Natella; Zhuk, Regina; Geenevasen, Jan A.; Van Den Burg, Alida; Koomen, Gerrit-Jan
Synthesis, 1999 , # 5 p. 775 - 778
