2,2'-二硫代二-嘧啶合成路线 (共 19 条)
反应条件
in chloroform
Ambient temperature; Title compound not separated from byproducts;
参考文献
Brzezinska, Ewa; Ternay, Andrew L.
Journal of Organic Chemistry, 1994 , vol. 59, # 26 p. 8239 - 8244
反应条件
in tetrahydrofuran
60 h; Ambient temperature;
参考文献
Davidson, Jack L.; Murray, Ian E. P.; Preston, Peter N.
Journal of Chemical Research, Miniprint, 1981 , # 5 p. 1601 - 1627
反应条件
T=180°C; Inert atmosphereAutoclave; Catalytic behavior;
参考文献
Corma, Avelino; Navas, Javier; Rodenas, Tania; Sabater, Maria J.
Chemistry - A European Journal, 2013 , vol. 19, # 51 p. 17464 - 17471
反应条件
in tert-butyl alcohol
0.75 h; or in THF, 45 min;
参考文献
Beadle, Charles D.; Bowman, W. Russell; Prousek, Josef
Tetrahedron Letters, 1984 , vol. 25, # 43 p. 4979 - 4982
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
23 h; Irradiation;
参考文献
Bowman, W. Russell; Rakshit, Devajvoti; Valmas, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2327 - 2336
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
18 h; Irradiation;
参考文献
Bowman, W. Russell; Rakshit, Devajvoti; Valmas, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2327 - 2336
反应条件
in methanol
0.166667 h; investigation of reaction with several thiolates with and without light, oxygen atmosphere and p-dinitrobenzene(p-DNB) or di-t-butylnitroxide (DTBN) in various solvents, deuterium labelling studies; Product distributionMechanism;
参考文献
Beadle, Charles D.; Bowman, W. Russell; Prousek, Josef
Tetrahedron Letters, 1984 , vol. 25, # 43 p. 4979 - 4982
反应条件
oxygen in N,N-dimethyl-formamide
8 h;
参考文献
Bowman, W. Russell; Rakshit, Devajvoti; Valmas, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2327 - 2336
反应条件
chlorine in dichloromethane
T=20°C; Chlorination;
参考文献
Miura; Tomimura; Teki
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7889 - 7895