反应条件
1: 86 percent / 1) isobutylmagnesium bromide / 1) Cp2TiCl2, 2) CuI / 1) ether, 0 to 25 deg C, 6 h., 2) THF, -30 to 25 deg C, 5 h.
2: 74 percent / oxygen / PdCl2, CuCl
3: m-chloroperbenzoic acid
4: methanol; H2SO4 / 13 h / Heating
View Scheme
参考文献
Sato, Fumie; Watanabe, Hiroshi; Tanaka, Youichi; Yamaji, Takafumi; Sato, Masao
Tetrahedron Letters, 1983 , vol. 24, # 10 p. 1041 - 1044
