(R)-1-苯基-2-丙醇合成路线 (共 57 条)
反应条件
(S)-HBTM; N-ethyl-N,N-diisopropylamine in 1,1-dimethylpropan-1-ol; toluene T=-40°C; 10 h; optical yield given as percent ee;
参考文献
Organic Letters, , vol. 10, # 6 p. 1115 - 1118
反应条件
1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 °C / |Inert atmosphere 2: lipase from candida antartica / aq. phosphate buffer / 48 h / 30 °C View Scheme
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 °C / |Inert atmosphere 2: lipase from candida antartica / aq. phosphate buffer / 48 h / 30 °C View Scheme
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
vinyl acetate; subtilisin in di-isopropyl ether T=10 - 40°C; resolution; Thermodynamic data;
参考文献
Chemistry Letters, , # 7 p. 782 - 783
反应条件
Sphingobium japonicum haloalkane dehalogenase T=21°C; pH=8.2; Tris sulfate bufferResolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 35 p. 6111 - 6115
反应条件
1: aq. H2SO4 2: (i) PBr5, CHCl3, (ii) Zn-Cu, aq. HCl View Scheme
参考文献
Chemische Berichte, , vol. 94, p. 893 - 901
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 53, # 23 p. 5531 - 5534
反应条件
24 h; Lactobacillus kefir; Yield given;
参考文献
Tetrahedron Asymmetry, , vol. 5, # 7 p. 1249 - 1268
反应条件
(i) PBr5, CHCl3, (ii) Zn-Cu, aq. HCl; Multistep reaction;
参考文献
Chemische Berichte, , vol. 94, p. 893 - 901
参考文献
Journal of the Chemical Society, , p. 1079