(E)-4',beta-二氯丙烯酰苯合成路线 (共 6 条)
反应条件
aluminium trichloride in chloroform 1.) 55-65 deg C, 24 h, 2.) 30 min;
参考文献
Reddy, D. Bhaskar; Babu, N. Chandrasekhar; Padmavathi; Sumathi
Synthesis, 1999 , # 3 p. 491 - 494
反应条件
carbon disulfide; aluminium trichloride
参考文献
Gryszkiewicz-Trochimowski; Schmidt; Gryszkiewicz-Trochimowski
Bulletin de la Societe Chimique de France, 1948 , p. 593,596
反应条件
diethyl ether; hydrazine hydrate
参考文献
Kotschetkow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 1181,1185; engl. Ausg. S. 1206, 1209
参考文献
Kotschetkow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 1181,1185; engl. Ausg. S. 1206, 1209
反应条件
1: 95.7 percent / tetrahydrofuran / 3 h / 20 °C 2: 94 percent / NEt3 / acetonitrile 3: 46 percent / 1-acetoxybuta-1,3-diene, hydroquinone / acetonitrile / 12 h / 50 °C View Scheme
参考文献
Katritzky, Alan R.; Rahimi-Rastgoo, Soheila; Sabongi, Gebran J.; Fischer, Gerhard W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 362 - 371
反应条件
1: benzene
2: ethanolic NaOH-solution; soda lime / 380 °C / unter vermindertem Druck
View Scheme
参考文献
Kotschetkow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1657; engl. Ausg. S. 1632