3-(4-甲氧基苄亚基)戊烷-2,4-二酮合成路线 (共 7 条)
反应条件
USY zeolite in benzene 2.3 h; Heating;
参考文献
Wang; Ma, YuDao; Zuo, BoJun
Synthetic Communications, 1997 , vol. 27, # 23 p. 4107 - 4110
反应条件
piperidine; cyclohexane in acetylacetone
参考文献
SYTHEON LIMITED
Patent: US2012/141395 A1, 2012 ;
反应条件
copper dichloride in tetrahydrofuran 120 h; Ambient temperature;
参考文献
Attanasi, Orazio; Filippone, Paolino; Mei, Amedeo
Synthetic Communications, 1983 , vol. 13, # 14 p. 1203 - 1208
反应条件
(i) THF*TiCl4, Py, CCl4, (ii) /BRN= 4157967/, DMF; Multistep reaction;
参考文献
Lehnert,W.
Synthesis, 1974 , p. 667 - 669
反应条件
triethylamine in ethanol Ambient temperature;
参考文献
Martin, Nazario; Seoane, Carlos; Soto, Jose L.
Tetrahedron, 1988 , vol. 44, # 18 p. 5861 - 5868
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; copper(l) chloride in acetonitrile
T=20°C; 0.5 h;
参考文献
Zhang, Lingjuan; Xu, Xianxiu; Shao, Qiu-Rong; Pan, Ling; Liu, Qun
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7393 - 7399
反应条件
in acetonitrile
T=37°C; two molar equivalents of dimethyl(methylene)ammonium chloride;
参考文献
Dimmock; Raghavan; Logan; Bigam
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 3 p. 248 - 254