8-羟基-5,7-二甲氧基-2-[(7E,9E,11E)-4-甲氧基-3,5,6,11-四甲基-7,9,11-十三碳三烯-1-基]-3-甲基-4H-苯并吡喃-4-酮合成路线 （共 31 条）
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 3 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
palladium diacetate; sodium carbonate in acetone
T=20°C; 2.5 h;
参考文献
Korolev; Bumagin
Russian Chemical Bulletin, 2004 , vol. 53, # 2 p. 364 - 369
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
sodium carbonate; palladium on activated charcoal in water
Suzuki reaction; 1 h; Heating;
参考文献
Lu, Gang; Franzen, Robert; Zhang, Qian; Xu, Youjun
Tetrahedron Letters, 2005 , vol. 46, # 24 p. 4255 - 4259
反应条件
sodium carbonate; palladium on activated charcoal in water
Suzuki reaction; 1 h; Heating;
参考文献
Lu, Gang; Franzen, Robert; Zhang, Qian; Xu, Youjun
Tetrahedron Letters, 2005 , vol. 46, # 24 p. 4255 - 4259
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=60°C; 3 h;
参考文献
Ciattini, Pier Giuseppe; Morera, Enrico; Ortar, Giorgio
Tetrahedron Letters, 1992 , vol. 33, # 33 p. 4815 - 4818
反应条件
in tetrahydrofuran
under inert atm. soln. NaBAr4 in THF was added dropwise at room temp. toBi(III) carboxylate in the same solvent and refluxed for 16 h; solvent was removed in vacuo, residue was extd. into hexane, filtered and subjected to column chromy. on silica (pentane-CH2Cl2 90:10);
参考文献
Stavila, Vitalie; Thurston, John H.; Prieto-Centurion, Dario; Whitmire, Kenton H.
Organometallics, 2007 , vol. 26, # 27 p. 6864 - 6866
反应条件
in tetrahydrofuran
under inert atm. soln. NaBAr4 in THF was added dropwise at room temp. toBi(III) carboxylate in the same solvent and refluxed for 16 h; solvent was removed in vacuo, residue was extd. into hexane, filtered and subjected to column chromy. on silica (pentane-CH2Cl2 90:10);
参考文献
Stavila, Vitalie; Thurston, John H.; Prieto-Centurion, Dario; Whitmire, Kenton H.
Organometallics, 2007 , vol. 26, # 27 p. 6864 - 6866
