in tetrahydrofuran byproducts: NaCl; Ar atmosphere, filtration of metal complex soln. through Kieselgur to a tube containing the solid ligand at 20°C; filtration (Kieselgur), evapn. to dryness, dissolution (THF), chromy. (silica gel, elution of byproducts with Et2O, elution of main product withTHF), removement of solvent (vacuum); elem. anal.;
参考文献
Kircher, Peter; Huttner, Gottfried; Heinze, Katja; Schiemenz, Berthold; Zsolnai, Laszlo; Buechner, Michael; Driess, Alexander
European Journal of Inorganic Chemistry, 1998 , # 6 p. 703 - 720
in n-heptane; toluene Kinetics; byproducts: CO; 25.0°C, 0.1-100 MPa;
参考文献
Cao, Shibai; Shi, Yanlong; Hollmann, Jens; Eldik, Rudi van; Eyring, Edward M.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1996 , p. 1629 - 1636
