in various solvent(s) T=393°C; Kinetics;

<b>Multi-step reaction with 5 steps<br /> </b>1.1: sodium azide; trifluoroacetic acid / chloroform / -10 &deg;C<br />2.1: ammonium formate; palladium 10 on activated carbon / ethanol / 50 &deg;C<br />3.1: sulfuryl dichloride; triethylamine / dichloromethane / -78 &deg;C<br />4.1: sodium hydride / tetrahydrofuran / 2 h / 0 &deg;C<br />4.2: -78 - 20 &deg;C<br />5.1: acetonitrile / 24 h / 50 &deg;C / |Inert atmosphere<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: isopentyl nitrite / diethyl ether / 0.08 h / |Inert atmosphere<br />1.2: 0.5 h / |Inert atmosphere<br />2.1: tetramethyl ammonium acetate; acetic acid / acetonitrile / 50 &deg;C / |Inert atmosphere<br /> <br /> &nbsp;