顺-1,2-环己基二甲醇合成路线 （共 25 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 2 h; Inert atmosphereReflux;
参考文献
Lee, Sunkyung; Song, Jong-Hwan; Park, Chul Min; Kim, Jin-Seok; Jeong, Ji-Hye; Cho, Woo-Young; Lim, Dong-Chul
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 11 p. 1054 - 1058
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Ambient temperature;
参考文献
Barry, Carey N.; Evans, Slayton A.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3361 - 3364
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Jackson, W. Roy; Perlmutter, Patrick; Tasdelen, E. Elizabeth
Journal of the Chemical Society, Chemical Communications, 1990 , # 10 p. 763 - 764
反应条件
1: LiAlH4 / diethyl ether 2: (hydrogenation) View Scheme
参考文献
Journal of the American Chemical Society, , vol. 86, p. 650 - 658
反应条件
methanol; potassium carbonate deacylation; 3 h; Heating;
参考文献
Chemistry - A European Journal, , vol. 5, # 6 p. 1905 - 1916
反应条件
tert.-butylhydroperoxide; [Fe(OTf)2-Py(ProMe)2] in decane; acetonitrile T=20°C; 0.5 h;
参考文献
Dalton Transactions, , # 31 p. 3365 - 3368
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the American Chemical Society, , vol. 94, p. 5017 - 5023
反应条件
1: H2 / 10percent Pd/C / ethanol / Ambient temperature 2: 1) NaIO4, 2) NaBH4 View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 3011 - 3015
反应条件
n-butyllithium; zirconocene dichloride; oxygen 1.)a) hexane, toluene, -78 deg C, 10 min, b) RT, 22 h, 2.) hexane, toluene, 0 deg C, 5 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 116, # 21 p. 9457 - 9463
反应条件
1: H2, tetrakis(acetato)dirhodium(II) (<Rh(OAc)2>2) / benzene / 25857.4 Torr 2: LAH / diethyl ether View Scheme
参考文献
Australian Journal of Chemistry, , vol. 45, # 5 p. 823 - 834
