顺-1,2-环己基二甲醇合成路线 （共 25 条）
反应条件
1: 74 percent / Et3N / diethyl ether / a) O dge C, 30 min, b) RT, 12 h 2: H2, tetrakis(acetato)dirhodium(II) (<Rh(OAc)2>2) / benzene / 25857.4 Torr 3: LAH / diethyl ether View Scheme
参考文献
Australian Journal of Chemistry, , vol. 45, # 5 p. 823 - 834
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the Chemical Society, , p. 399,402
Journal of Organic Chemistry, , vol. 19, p. 1449,1461
参考文献
Journal of the American Chemical Society, , vol. 86, p. 650 - 658
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Organic Magnetic Resonance, , vol. 16, # 4 p. 261 - 265
反应条件
lithium aluminium tetrahydride
参考文献
Tetrahedron Letters, , vol. 26, # 17 p. 2073 - 2076
反应条件
sodium tetrahydroborate; sodium periodate Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 3011 - 3015
反应条件
1: 80 percent / NAD+, FMN, pH 9, HLADH, NaOH, glycine / Ambient temperature 2: 34 percent / NaOH / H2O / 192 h / 130 °C 3: 80 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme
参考文献
Jakovac, Ignac J.; Goodbrand, H. Bruce; Lok, Kar P.; Jones, J. Bryan
Journal of the American Chemical Society, 1982 , vol. 104, # 17 p. 4659 - 4665
反应条件
ammonium hydroxide; 2-ketoadipate monosodium salt in hexane 96 h; Ambient temperatureenzymatic reaction: (glutamate dehydrogenase (GluDH), horse liver alcohol dehydrogenase (HLADH), triphosphopyridine nucleotide sodium salt (NAD));
参考文献
Journal of Organic Chemistry, , vol. 51, # 12 p. 2388 - 2389
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethylsulfoxide-d6
T=23°C; Mechanism;
参考文献
Corey; Palani, Anandan
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 7945 - 7948
反应条件
in dimethylsulfoxide-d6
T=23°C; var. primary and secondary alcohol; Mechanism;
参考文献
Corey; Palani, Anandan
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 7945 - 7948
