(S)-1-(叔-丁基二甲基硅烷基氧基)-2-丁胺合成路线 （共 7 条）
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol P=760 Torr; 6 h;
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1H-imidazole in dichloromethane T=0 - 25°C;
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1: 88 percent / hydrogen; triethylamine / Pd/C / methanol / 12 h / 760 Torr 2: 95 percent / pyridine / 0 - 25 °C 3: 75 percent / sodium azide / dimethylformamide / 30 h / 60 °C 4: 95 percent / hydrogen; triethylamine / Pd/C / methanol / 6 h / 760 Torr View Scheme
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1: 75 percent / sodium azide / dimethylformamide / 30 h / 60 °C 2: 95 percent / hydrogen; triethylamine / Pd/C / methanol / 6 h / 760 Torr View Scheme
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1: 95 percent / pyridine / 0 - 25 °C 2: 75 percent / sodium azide / dimethylformamide / 30 h / 60 °C 3: 95 percent / hydrogen; triethylamine / Pd/C / methanol / 6 h / 760 Torr View Scheme
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Barker, Timothy J.; Jarvo, Elizabeth R.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 36 p. 8325 - 8328
反应条件
pyridine in dichloromethane
T=0 - 25°C;
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
