N-苄基-对甲苯磺酸胺合成路线 （共 161 条）
反应条件
1.1: NaH / tetrahydrofuran / 1 h / 0 °C 1.2: tetrahydrofuran / 0 - 20 °C 2.1: 87 percent / SmI2 / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Tetrahedron, , vol. 56, # 7 p. 979 - 988
反应条件
1: aqueous alcoholic alkaline solution 2: concentrated hydrochloric acid / 165 - 170 °C 3: nitric acid / 100 °C View Scheme
参考文献
Holmes; Ingold
Journal of the Chemical Society, 1925 , vol. 127, p. 1810
反应条件
1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C -> 0 deg C, 30 min, 2.) THF, hexane, -78 deg C -> rt, overnight 2: 1.) Li, naphthalene, 2.) H2O / 1.) THF, -78 deg C, 2 h View Scheme
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1997 , vol. 53, # 42 p. 14355 - 14368
反应条件
[bis(acetoxy)iodo]benzene; iodine in 1,2-dichloro-ethane T=30 - 40°C; 6 h; ultrasonic irradiation;
参考文献
Katohgi, Masashi; Togo, Hideo
Tetrahedron, 2001 , vol. 57, # 35 p. 7481 - 7486
反应条件
1: 1) 2,1N alcoh. KOH / 1) heating, 2) CH3COCH3, -50 deg C, 1 h; 4 h, r.t. View Scheme
参考文献
Fuhrmann, J.; Haber, H.; Haupt, M.; Henning, H.-G.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 6 p. 1055 - 1059
反应条件
1: aqueous alcoholic NaOH-solution 2: concentrated hydrochloric acid / 180 °C View Scheme
参考文献
Carothers; Bickford; Hurwitz
Journal of the American Chemical Society, 1927 , vol. 49, p. 2908
反应条件
1: aqueous alcoholic NaOH-solution / durch Propylierung 2: concentrated hydrochloric acid / 180 °C View Scheme
参考文献
Carothers; Bickford; Hurwitz
Journal of the American Chemical Society, 1927 , vol. 49, p. 2908
反应条件
1: 99 percent / DMAP / tetrahydrofuran / 20 °C 2: 96 percent / hydrogen / Pearlman's catalyst / ethanol / 760.05 Torr View Scheme
参考文献
Johnson II, David C.; Widlanski, Theodore S.
Tetrahedron Letters, 2004 , vol. 45, # 46 p. 8483 - 8487
反应条件
DBN in acetonitrile T=80°C; 16 h; Inert atmosphere;
参考文献
Taylor, James E.; Jones, Matthew D.; Williams, Jonathan M. J.; Bull, Steven D.
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2808 - 2818
反应条件
zinc(II) chloride T=20°C; 0.0833333 h;
参考文献
Raji Reddy, Chada; Mahipal, Bodugam; Yaragorla, Srinivasa Rao
Tetrahedron Letters, 2007 , vol. 48, # 42 p. 7528 - 7532
