5-硝基-1H-吲哚-2-羧酸甲酯合成路线 （共 12 条）
反应条件
in toluene T=200°C; 0.166667 h; Microwave irradiation;
参考文献
Ranasinghe, Nadeesha; Jones, Graham B.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1740 - 1742
反应条件
manganese(IV) oxide in toluene 1 h; Heating;
参考文献
Lavrenov, Sergei N.; Lakatosh, Sergei A.; Lysenkova, Ludmila N.; Korolev, Alexander M.; Preobrazhenskaya, Maria N.
Synthesis, 2002 , # 3 p. 320 - 322
反应条件
1: 97 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH2Cl2 / 2 h / 20 °C 2: 34 percent / K2CO3; L-proline / CuI / dioxane / 24 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 51 p. 8877 - 8880
反应条件
hydrogenchloride T=20°C;
参考文献
Journal of Medicinal Chemistry, , vol. 48, # 14 p. 4511 - 4525
反应条件
1: Et3N / 1 h / 20 °C 2: 750 mg / Ac2O; HNO3 / 1.5 h / 0 °C 3: aq. HCl / Heating 4: 350 mg / SOCl2 / 20 °C 5: 78 percent / γ-MnO2 / toluene / 1 h / Heating View Scheme
参考文献
Synthesis, , # 3 p. 320 - 322
反应条件
1: H2SO4; HNO3 / 0.5 h / -20 - -10 °C 2: 350 mg / SOCl2 / 20 °C 3: 78 percent / γ-MnO2 / toluene / 1 h / Heating View Scheme
参考文献
Synthesis, , # 3 p. 320 - 322
反应条件
1: 750 mg / Ac2O; HNO3 / 1.5 h / 0 °C 2: aq. HCl / Heating 3: 350 mg / SOCl2 / 20 °C 4: 78 percent / γ-MnO2 / toluene / 1 h / Heating View Scheme
参考文献
Synthesis, , # 3 p. 320 - 322
反应条件
1: 350 mg / SOCl2 / 20 °C 2: 78 percent / γ-MnO2 / toluene / 1 h / Heating View Scheme
参考文献
Synthesis, , # 3 p. 320 - 322
反应条件
1: aq. HCl / Heating 2: 350 mg / SOCl2 / 20 °C 3: 78 percent / γ-MnO2 / toluene / 1 h / Heating View Scheme
参考文献
Synthesis, , # 3 p. 320 - 322
反应条件
1: sodium / methanol / 12 h / -20 - 0 °C 2: anhydrous xylene / 1 h / Reflux View Scheme
参考文献
Archives of Pharmacal Research, , vol. 34, # 3 p. 357 - 367
