(2-溴-3-噻吩基)甲胺合成路线 (共 3 条)
反应条件
hydrazine hydrate in methanol 1 h, room temperature, reflux, 10 min;
参考文献
Finch, Harry; Reece, Donald H.; Sharp, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 9 p. 1193 - 1204
反应条件
1: 81 percent / NBS, (PhCO)2O2 / CCl4 / 3 h / Heating 2: 79 percent / dimethylformamide / room temperature, 90 min, 45 deg C, 90 min 3: 55 percent / N2H4*H2O / methanol / 1 h, room temperature, reflux, 10 min View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 1193 - 1204
反应条件
1: 79 percent / dimethylformamide / room temperature, 90 min, 45 deg C, 90 min 2: 55 percent / N2H4*H2O / methanol / 1 h, room temperature, reflux, 10 min View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 1193 - 1204