反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78°C; 2 h; Inert atmosphere; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1697939', constants.ctx, '0')">boric acid trimethyl ester</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78 - 20°C; 12 h; Inert atmosphere; <br />
参考文献
Zhai, Linyi; Shukla, Ruchi; Wadumethrige, Shriya H.; Rathore, Rajendra Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4748 - 4760
