4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane 2.5 h;
参考文献
Satcharoen, Vachiraporn; McLean, Neville J.; Kemp, Stephen C.; Camp, Nicholas P.; Brown, Richard C. D.
Organic Letters, 2007 , vol. 9, # 10 p. 1867 - 1869
1: oxalyl chloride, DMF / benzene / 0.5 h / Ambient temperature
2: pyridine / benzene / 0.5 h / Ambient temperature
3: benzene / Irradiation; various reaction conditions; also with 1,4-cyclohexadiene
View Scheme
参考文献
Davies, Alwyn G.; Sutcliffe, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 819 - 824