(S)-4-(2-甲基硫代乙基)恶唑-2,5-二酮合成路线 (共 6 条)
反应条件
carbon in tetrahydrofuran T=55°C; 0.5 h;
参考文献
Katakai, Ryoichi; Iizuka, Yasuko
Journal of Organic Chemistry, 1985 , vol. 50, # 5 p. 715 - 716
反应条件
phosphorus tribromide in diethyl ether 2 h; Ambient temperature;
参考文献
Itoh, Osamu; Amano, Akira
Synthesis, 1999 , # 3 p. 423 - 428
反应条件
1: With acetic acid in acetonitrile T=80°C; Inert atmosphere; 2: With hydrogenchloride in water; acetonitrile T=20°C; 1 h; Inert atmosphere;
参考文献
Koga, Koichi; Sudo, Atsushi; Endo, Takeshi
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 19 p. 4351 - 4355
反应条件
in tetrahydrofuran; toluene T=50°C; 3 h; Inert atmosphere;
参考文献
Kramer, Jessica R.; Deming, Timothy J.
Biomacromolecules, 2012 , vol. 13, # 6 p. 1719 - 1723
反应条件
in tetrahydrofuran 2.5 h; RefluxInert atmosphere;
参考文献
Ronga, Luisa; Verdie, Pascal; Sanchez, Pierre; Enjabal, Christine; Maurras, Amelie; Jullian, Magalie; Puget, Karine; Martinez, Jean; Subra, Gilles
Amino Acids, 2013 , vol. 44, # 2 p. 733 - 742
反应条件
triethylamine in water
参考文献
Gait,R.J. et al.
Canadian Journal of Chemistry, 1972 , vol. 50, p. 299 - 303