2,5-二(三甲基硅烷基)-呋喃合成路线 (共 5 条)
反应条件
tetrabutylammomium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide electrochemical conditions (Mg anode, 2.2 F.mol-1); Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 570, # 1 p. 147 - 154
反应条件
tetrabutylammomium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide electrochemical conditions (Al anode, 2.2 F.mol-1); Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 570, # 1 p. 147 - 154
反应条件
n-butyllithium 1.) ether, hexane; Multistep reaction;
参考文献
Bock, H.; Roth, B.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 14, p. 211 - 224
反应条件
calcium 1.5 h; Ambient temperature;
参考文献
Mochida, Kunio; Kojima, Kenji; Yoshida, Yasuhiro
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2255 - 2256
反应条件
1: 84 percent / pentane / 2 h / -78 °C / Irradiation
2: H2 / Pd
View Scheme
参考文献
Barton; Hussmann
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6316 - 6318