二(呋喃-2-基)-二甲基硅烷合成路线 (共 14 条)
反应条件
1: furan With n-butyllithium in hexane 1 h; Heating; 2: dimethyl-dichlorosilane in hexane T=20°C;
参考文献
Neugebauer, Peter; Klingebiel, Uwe; Noltemeyer, Mathias
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 10 p. 913 - 923
反应条件
tetrabutylammomium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide 2:1 substrate/Me2SiCl2 ratio, electrochemical conditions (Mg anode, 2.2 F.mol-1);
参考文献
Moreau, Carole; Serein-Spirau, Francoise; Bordeau, Michel; Biran, Claude
Journal of Organometallic Chemistry, 1998 , vol. 570, # 1 p. 147 - 154
反应条件
tetrabutylammomium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide electrochemical conditions (Mg anode, 2.2 F.mol-1);
参考文献
Moreau, Carole; Serein-Spirau, Francoise; Bordeau, Michel; Biran, Claude
Journal of Organometallic Chemistry, 1998 , vol. 570, # 1 p. 147 - 154
反应条件
in diethyl ether; hexane T=-30 - 25°C;
参考文献
Lukevics, E.; Gevorgyan, V. N.; Goldberg, Y. S.; Shymanska, M. V.
Journal of Organometallic Chemistry, 1985 , vol. 294, p. 163 - 172
反应条件
1: 21 percent Chromat. / tetrahydrofuran; hexane / 1 h / -30 - 25 °C 2: tetrahydrofuran; hexane / 1 h / -30 - 25 °C View Scheme
参考文献
Gevorgyan, Vladimir; Borisova, Larisa; Lukevics, Edmunds
Journal of Organometallic Chemistry, 1992 , vol. 441, # 3 p. 381 - 387
反应条件
tetrabutylammomium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide electrochemical conditions (Mg anode, 4.4 F.mol-1);
参考文献
Moreau, Carole; Serein-Spirau, Francoise; Bordeau, Michel; Biran, Claude
Journal of Organometallic Chemistry, 1998 , vol. 570, # 1 p. 147 - 154
反应条件
furan-2-yl-lithium in tetrahydrofuran; hexane T=-30 - 25°C; 1 h;
参考文献
Gevorgyan, Vladimir; Borisova, Larisa; Lukevics, Edmunds
Journal of Organometallic Chemistry, 1992 , vol. 441, # 3 p. 381 - 387
反应条件
in tetrahydrofuran; hexane T=-30 - 25°C; 1 h;
参考文献
Gevorgyan, Vladimir; Borisova, Larisa; Lukevics, Edmunds
Journal of Organometallic Chemistry, 1992 , vol. 441, # 3 p. 381 - 387
反应条件
in tetrahydrofuran; hexane T=-30 - 25°C; 1 h;
参考文献
Gevorgyan, Vladimir; Borisova, Larisa; Lukevics, Edmunds
Journal of Organometallic Chemistry, 1992 , vol. 441, # 3 p. 381 - 387
反应条件
in tetrahydrofuran; hexane T=-30 - 25°C; 1 h;
参考文献
Gevorgyan, Vladimir; Borisova, Larisa; Lukevics, Edmunds
Journal of Organometallic Chemistry, 1992 , vol. 441, # 3 p. 381 - 387