3-(Fmoc-氨基)-1-丙醇合成路线 (共 5 条)
反应条件
sodium hydrogencarbonate in 1,4-dioxane T=0 - 20°C;
参考文献
Nasopoulou, Magdalini; Georgiadis, Dimitris; Matziari, Magdalini; Dive, Vincent; Yiotakis, Athanasios
Journal of Organic Chemistry, 2007 , vol. 72, # 19 p. 7222 - 7228
反应条件
in 1,4-dioxane; water T=20°C; 16 h;
参考文献
Crestey, Francois; Ottesen, Lars K.; Jaroszewski, Jerzy W.; Franzyk, Henrik
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 5890 - 5893
反应条件
in dichloromethane T=20°C; 0.0833333 h;
参考文献
Shimizu, Mamoru; Sodeoka, Mikiko
Organic Letters, 2007 , vol. 9, # 25 p. 5231 - 5234
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate T=80°C;
参考文献
More, Jesse D.; Finney, Nathaniel S.
Organic Letters, 2002 , vol. 4, # 17 p. 3001 - 3003
反应条件
sodium hydroxide; triphenylphosphine; diethylazodicarboxylate
1.) THF, 3 h; 2.) 10 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Krchnak, Viktor; Flegelova, Zuzka; Weichsel, Aleksandra S.; Lebl, Michal
Tetrahedron Letters, 1995 , vol. 36, # 35 p. 6193 - 6196