1: With AlCl3, aluminium chloride in dichloromethane T=0 - 5°C; Friedel Crafts Acylation; 1.5 h; 2: With hydrogenchloride in dichloromethane; water T=0°C;
1: With sodium disulfite in water
T=85°C; 0.166667 h;
2: With sodium hydroxide in water; isopropyl alcohol
0.25 h; Reflux; Product distribution / selectivity;
参考文献
Meneguzzo, Enzo; Norcini, Gabriele; Li Bassi, Giuseppe
Patent: US2011/65962 A1, 2011 ;
Location in patent: Page/Page column 5 ;
