环对甲基亚苄基丙二酸-2,2-丙二醇合成路线 （共 16 条）
反应条件
dihydrogen peroxide in acetonitrile
72 h; Ambient temperature; Yields of byproduct given;
参考文献
Tsuno, Takashi; Sugiyama, Kunio; Ago, Hideo
Heterocycles, 1994 , vol. 38, # 12 p. 2631 - 2654
反应条件
in N,N-dimethyl-formamide
T=10°C; 0.25 h;
参考文献
Izquierdo, M. L.; Arenal, I.; Bernabe, M.; Alvarez, E. Fernandez
Tetrahedron, 1985 , vol. 41, # 1 p. 215 - 220
反应条件
in methanol; diethyl ether
T=-70°C; 1 h;
参考文献
Izquierdo, M. L.; Arenal, I.; Bernabe, M.; Alvarez, E. Fernandez
Tetrahedron, 1985 , vol. 41, # 1 p. 215 - 220
反应条件
1: 92 percent / diethyl ether / 0.83 h / 0 - 20 °C
2: 85 percent / pyridine / CH2Cl2 / 7 h / 0 - 20 °C
3: 5 h / Heating
4: aq. NaOH / ethanol / 6 h / Heating
View Scheme
参考文献
Mahulikar; Mane
Journal of Chemical Research, 2006 , # 1 p. 15 - 18
反应条件
1: 92 percent / diethyl ether / 0.83 h / 0 - 20 °C
2: 92 percent / pyridine / H2O / 6 h / Heating
View Scheme
参考文献
Mahulikar; Mane
Journal of Chemical Research, 2006 , # 1 p. 15 - 18
反应条件
in diethyl ether
T=0 - 20°C; 0.833333 h;
参考文献
Mahulikar; Mane
Journal of Chemical Research, 2006 , # 1 p. 15 - 18
