二(4-叔丁基苯基)甲酮合成路线 （共 26 条）
反应条件
chromium(VI) oxide; sulfuric acid; water in acetone Inert atmosphere;
参考文献
Tetrahedron, , vol. 65, # 16 p. 3062 - 3068
反应条件
1: 87 percent / Grignard reaction 2: 94 percent / SOCl2 / diethyl ether / Heating 3: 18 percent / tributylamine, oxygen / various solvent(s) / 6.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 769 - 778
反应条件
1: 94 percent / SOCl2 / diethyl ether / Heating 2: 18 percent / tributylamine, oxygen / various solvent(s) / 6.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 769 - 778
反应条件
(i) LiH, 1,2-dimethoxy-ethane, (ii) /BRN= 3934304/, Et2O; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 95, p. 8118 - 8133
反应条件
tributyl-amine in various solvent(s) 17 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 769 - 778
反应条件
n-butyllithium 1) Et2O, hexane, -78 deg C, 2h, 2a) Et2O, -78 deg C, 30 min, 2b) RT, 6h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 12 p. 1179 - 1182
反应条件
thionyl chloride 1) THF, pentane, -78 deg C, 30 min, 2a) -78 deg C, 30 min, 2b) RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthesis, , # 12 p. 1179 - 1182
反应条件
aluminium trichloride
参考文献
Journal of the Chemical Society, , p. 790,793
反应条件
(i) 1,1-diphenyl-ethyl hydroperoxide, Na2CO3, (ii) H2SO4; Multistep reaction;
参考文献
Sov. Prog. Chem. (Engl. Transl.), , vol. 34, # 3 p. 280 - 284,38 - 40
反应条件
1: (electrolysis) 2: (electrolysis) View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 33, p. 735 - 741
