反应条件
1: 1) O3, O2, 2) LiAlH4 / 1) CH2Cl2, -78 deg C, 2a) THF, RT, 0.5 h, 2b) reflux, 1 h 2: 80 percent / p-TsOH / nitromethane / 1.2 h / Ambient temperature 3: 88 percent / Jones reagent / acetone / 0 °C 4: 71 percent / KOH, N2H4*H2O / various solvent(s) / 1 h / Heating View Scheme
参考文献
Barrero, Alejandro F.; Altarejos, Joaquin; Alvarez-Manzaneda, Enrique J.; Ramos, Jose M.; Salido, Sofia
Tetrahedron, 1993 , vol. 49, # 28 p. 6251 - 6262
