4-[2,2’:6’,2"-三联吡啶]-4’-基-苯甲酸合成路线 （共 7 条）
反应条件
1: With ammonium hydroxide; potassium hydroxide in methanol T=20°C; 72 h; 2: With hydrogenchloride in methanol; water pH=2;
参考文献
Stublla, Arta; Potvin, Pierre G.
European Journal of Inorganic Chemistry, 2010 , # 19 p. 3040 - 3050
反应条件
sodium hydroxide in methanol 24 h; Heating;
参考文献
Duprez, Virginie; Krebs, Frederik C.
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3785 - 3789
反应条件
sodium hydroxide; ammonia in ethanol; water T=20°C; 17 h;
参考文献
Constable, Edwin C.; Dunphy, Emma L.; Housecroft, Catherine E.; Neuburger, Markus; Schaffner, Silvia; Schaper, Frank; Batten, Stuart R.
Dalton Transactions, 2007 , # 38 p. 4323 - 4332
反应条件
hydrogenchloride in water pH=4 - 5; Inert atmosphere;
参考文献
Manner, Virginia W.; Mayer, James M.
Journal of the American Chemical Society, 2009 , vol. 131, # 29 p. 9874 - 9875
反应条件
potassium dichromate; sulfuric acid; water; nitric acid T=160°C; 36 h;
参考文献
Kelly, Niamh R.; Goetz, Sandrine; Hawes, Chris S.; Kruger, Paul E.
Tetrahedron Letters, 2011 , vol. 52, # 9 p. 995 - 998
反应条件
1: 34 percent / piperidine; acetic acid / methanol / 5 h / Heating 2: 64 percent / ammonium acetate / methanol / 4 h / Heating 3: 80 percent / NaOH / methanol / 24 h / Heating View Scheme
参考文献
Duprez, Virginie; Krebs, Frederik C.
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3785 - 3789
反应条件
1: 64 percent / ammonium acetate / methanol / 4 h / Heating 2: 80 percent / NaOH / methanol / 24 h / Heating View Scheme
参考文献
Duprez, Virginie; Krebs, Frederik C.
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3785 - 3789
